HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → N-(5-bromo-3-pyridyl)-N'-cyano-N"-(2-phenylthioethyl)guanidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Phenyl-2-aminoethyl sulfide | HCID 37013 | — |
| Reactant | HCID 178503895 | HCID 178503895 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | N-(5-bromo-3-pyridyl)-N'-cyano-N"-(2-phenylthioethyl)guanidine | HCID 54221473 | — |
Reaction Steps
S-Methyl N-(5-bromo-3-pyridyl)-N'-cyanoisothiourea (650 mg) and 2-phenylthioethylamine (740 mg) in pyridine (0.5 ml) were heated to 50° C. for 5 hours. To the resulting clear solution was added ether (10 ml), and the desired pure compound was collected by filtration and washed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05563160 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-262f92ccf08e488884e77e502fc46488 |
| Source note | uspto-grants-1996_10 |