HRID864510

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCN(CC)CCN1c2cc(Cl)ccc2S[C@H]2[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](CN=[N+]=[N-])O[C@H]21

HCID86749915

未命名化合物

PRODUCTS

生成物

结构：CCN(CC)CCN1c2cc(Cl)ccc2S[C@H]2[C@@H](O)[C@H](O)[C@@H](CN=[N+]=[N-])O[C@H]21

HCID86749917

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID222

Ammonia gas

H3N

PROCEDURE

实验过程

The compound (37) 10.1 g obtained in Example 36 was dissolved in 250 ml of ammonia-saturated methanol, and the solution was stirred for 6 hours at room temperature. The solvent was removed under reduced pressure to obtain the title compound quantitatively.

WORKUP

后处理

customThe solvent was removed under reduced pressure