2-(Dimethylamino)ethanol → Carbonic acid, bis[2-(dimethylamino)ethyl] ester

HRID 864665Notes

Reaction equation

HRID 864665 reaction equation
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[C:7](=O)([O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])[O:8]C(C)C>C(O)(C)C>[C:7](=[O:8])([O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])[O:6][CH2:5][CH2:4][N:2]([CH3:3])[CH3:1]

Participants

4

Reactant 2

HCID 79022-(Dimethylamino)ethanolHCID 19419881Isopropyl 2-dimethylaminoethyl carbonate

Product 1

HCID 76417Carbonic acid, bis[2-(dimethylamino)ethyl] ester

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

wherein the 2-(N,N-dimethylamino)ethanol reacts with the isopropyl 2-dimethylaminoethyl carbonate formed in step ii) to form bis[2-(N,N-dimethylamino)ethyl] carbonate and isopropanol,

Sources & evidence

ORD record
ord-57d425b02b5c439d9809caf8f30b7f3e
Source dataset
uspto-grants-1996_10
Patent number
US05563288

Reaction notes

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