2-(Dimethylamino)ethanol → Carbonic acid, bis[2-(dimethylamino)ethyl] ester

HRID 864671Notes

Reaction equation

HRID 864671 reaction equation
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[C:7](=O)([O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])[O:8]C(C)C>C(O)(C)C>[CH3:1][N:2]([CH2:4][CH2:5][O:6][C:7](=[O:8])[O:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16])[CH3:3]

Participants

4

Reactant 2

HCID 79022-(Dimethylamino)ethanolHCID 19419881Isopropyl 2-dimethylaminoethyl carbonate

Product 1

HCID 76417Carbonic acid, bis[2-(dimethylamino)ethyl] ester

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

wherein the 2-(N,N-dimethylamino)ethanol reacts with the isopropyl 2-dimethylaminoethyl carbonate formed in step ii) to form bis[2-(N,N-dimethylamino)ethyl]carbonate and isopropanol,

Sources & evidence

ORD record
ord-1870485b4f98448ebf76fab614703345
Source dataset
uspto-grants-1996_10
Patent number
US05563288

Reaction notes

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