Hydrazine → HCID 23374876, compound

Participants

Reaction Steps

A mixture of 1,3-diphthalimido-2-(t-butylcarboxymethyl)oxapropane(0.50 g, 1.08 mmol) and 55% hydrazine (0.23 mL, 4.6 mmol) in 2 mL of methanol is refluxed for 4 hrs. After cooling the reaction solution to room temperature, the solids are filtered and the filtrate is evaporated under reduced pressure to yield 1,3-diamino-2-(t-butylcarboxymethyl)oxapropane.

Provenance & Evidence