HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19417346, compound → HCID 136032772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19417346 | HCID 19417346 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 136032772 | HCID 136032772 | 101.6% |
Reaction Steps
To a solution of the product of step (c) (0.387 g) in 8 ml dioxane was added 110 mg of 10% palladium on carbon (Degussa type, water wet). The mixture was then shaken for 5 hours, filtered and the filter cake washed. The solvents were evaporated to yield 260 mg of 4-hydroxy-3-(3-ethoxy-2-methyl-4-methylsulfonylbenzoyl)pyrid-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05565413 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-266f74485d184b209512ccbf58229e1c |
| Source note | uspto-grants-1996_10 |