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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 864895Generated: October 30, 2026

HCID 19417346, compound → HCID 136032772, compound

https://huagongshe.com/reaction/864895

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19417346HCID 19417346—
CatalystPalladiumHCID 23938—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 136032772HCID 136032772101.6%

Reaction Steps

To a solution of the product of step (c) (0.387 g) in 8 ml dioxane was added 110 mg of 10% palladium on carbon (Degussa type, water wet). The mixture was then shaken for 5 hours, filtered and the filter cake washed. The solvents were evaporated to yield 260 mg of 4-hydroxy-3-(3-ethoxy-2-methyl-4-methylsulfonylbenzoyl)pyrid-2-one.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05565413
Source datasetuspto-grants-1996_10
ORD IDord-266f74485d184b209512ccbf58229e1c
Source noteuspto-grants-1996_10