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4-Chlorophenyl Isocyanate → N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| 反応物 | 4-(Morpholin-4-yl)benzene-1-sulfonamide | HCID 735435 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | N-[[(4-chlorophenyl) amino]-carbonyl]-4-(4-morpholinyl) benzenesulfonamide | HCID 15345719 | — |
反応手順
4-Chlorophenylisocyanate (2.61 g, 17 moles) was dissolved in 16 ml of acetone and was then added dropwise to the sulfonamide solution. The mixture was then stirred overnight at room temperature, resulting in the formation of a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05565494 |
| 出典データセット | uspto-grants-1996_10 |
| ORD ID | ord-fdccf3362d874d0bba3eb0d86506ba63 |
| 出典メモ | uspto-grants-1996_10 |