HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 10176704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Benzene, 1-chloro-2,3,4-trifluoro- | HCID 142097 | — |
| Product | HCID 10176704 | HCID 10176704 | — |
Reaction Steps
If 0.15 mol of 2,3,4-trifluorochlorobenzene in 50 g of 100% strength sulfuric acid as diluent is used and nitration is carried out with 30.5 g (0.165 mol) of mixed acid prepared from 68.8% by weight of 100% strength H2SO4 and 31.2% by weight of 100% strength HNO3 at from 5° to 12° C., then reaction is complete after metered addition for 1 hour followed by stirring for an additional hour. The result is essentially the same.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05565612 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-dbd063c3d7ad4b13885891df3738961a |
| Source note | uspto-grants-1996_10 |