HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10717394, compound → HCID 10568249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10717394 | HCID 10717394 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 10568249 | HCID 10568249 | — |
Reaction Steps
A stirring solution of 2-t-butoxycarbonylamino-3-(1H-indol-3-yl)-N-(2-chlorobenzyl)propanamide (6.00 g, 14 mmol) in 30 ml of 70% aqueous trifluoroacetic acid (21 ml trifluoroacetic acid, 9 ml water) was allowed to stir overnight at room temperature. The progress of this deprotection reaction was monitored by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05565568 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-fb76ecefa60b42558d815dea2563f087 |
| Source note | uspto-grants-1996_10 |