HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-amino-1-piperidinecarboxylate → HCID 23374509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-amino-1-piperidinecarboxylate | HCID 100867 | — |
| Reactant | 4-Ethoxy-3-nitropyridine | HCID 356305 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 23374509 | HCID 23374509 | — |
Reaction Steps
A mixture of ethyl 4-amino-1-piperidinecarboxylate (3.53 g, 20.5 mmol) and 4-ethoxy-3-nitropyridine (3.65 g, 21/7 mmol) in CH3CN (25 mL) was heated at reflux for 40 hours. The reaction mixture was cooled to ambient temperature and concentrated in vacuo to give an orange syrup which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05567711 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-5b8ae9819dc8446a9b95b612a6523f32 |
| Source note | uspto-grants-1996_10 |