HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54426295, compound → Methyl 3-(5-methyl-2-furanyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54426295 | HCID 54426295 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3-(5-methyl-2-furanyl)propionate | HCID 14906307 | 107.1% |
Reaction Steps
A mixture of ethyl β-(5-methyl-2-furanyl)acrylate (8 g) in methanol (200 mL) and 1.5 g of 5% palladium on carbon was placed on a Paar hydrogenator and hydrogenated with H2. Palladium on carbon was filtered off by passing the reaction mixture through Super-Cel™ (filter agent) and the residue was washed with ethanol. The filtrate was concentrated in vacuo to yield 8 g of methyl 3-(5-methyl-2-furanyl)propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05567717 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-02ed42084638468ba10b2742216dcfa8 |
| Source note | uspto-grants-1996_10 |