Phenyl isocyanate → HCID 86749947, compound

HRID 865725Notes

Reaction equation

C1([N:7]=[C:8]=[O:9])C=CC=CC=1.[C:10]([O-:23])(=[O:22])[CH2:11][CH2:12][CH2:13]CCCCCCCC.[C:24]([O-:37])(=[O:36])[CH2:25][CH2:26][CH2:27]CCCCCCCC.C([Sn+2]CC[CH2:45][CH3:46])CCC>>[C:10]([OH:23])(=[O:22])[CH2:11][C:12]([CH3:13])=[O:9].[C:24]([OH:37])(=[O:36])[CH2:25][C:26]([CH3:27])=[O:9].[CH2:24]([C:11]([CH2:10][OH:23])([CH2:8][OH:9])[CH2:12][CH3:13])[OH:36].[NH2:7][C:8]([O:9][CH2:45][CH3:46])=[O:22]

Participants

Reactant 2

HCID 7672Phenyl isocyanate

HCID 9809426Di-n-butyldilauryltin

Product 1

HCID 86749947HCID 86749947, compound

Procedure

800 g of the above product were mixed with 100 g of phenyl isocyanate and 0.1 g of dibutyltin dilaurate and heated at 50° C. until the NCO content reached zero.

Sources & evidence

ORD record: ord-7ac04a9b586440658ef40f64d360d819
Source dataset: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05567761

Reaction notes

Loading…