Dichloromethane → HCID 23374674, compound

Participants

Reaction Steps

Compound 32 was prepared as described for 29. The reagents used were as follows, compound 26 (g, mol.), tetrafluoroboric acid-diethyl ether complex ml of a 54% solution in diethyl ether), dichloromethane (100 ml) and excess potassium carbonate. the final yield was a colorless liquid (g, %), (bpt. °C., torr.): 1H-NMR (CDCl3), d, (ppm). Mass spectroscopy, m/e M+.

Provenance & Evidence