HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl mercaptan → HCID 525387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl mercaptan | HCID 6387 | — |
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Product | HCID 525387 | HCID 525387 | 86% |
Reaction Steps
The title compound was prepared from isoamyl bromide and tert-butyl mercaptan according to the method of Example 1, 86% yield, bp 55°-56° C./7 mm Hg, n20D=1.4460; 1H NMR (CDCl3) δ 0.92 (d, J=6 Hz, 6H, CH3), 1.32 (s, 9H, CH3), 1.45 (q, 2H, CH2), 1.68 (septet, 1H, CH), 2.52 (t, J =6 Hz, 2H, CH2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05567849 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-4699e2e8629f4d3eacfbfc5cb8c6ec96 |
| Source note | uspto-grants-1996_10 |