HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 19963160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 21849844 | HCID 21849844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19963160 | HCID 19963160 | — |
Reaction Steps
After repetition of the previous steps, a mixture of 7-chloro-4-(3'-methylanilino)-6-nitroquinazoline (10.5 g), an ethanolic solution of methylamine (30% weight/volume; 100 ml) and ethanol (100 ml) was stirred at ambient temperature for 16 hours. The mixture was evaporated to give 7-methylamino-4-(3'-methylanilino)-6-nitroquinazoline which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05569658 |
| Source dataset | uspto-grants-1996_10 |
| ORD ID | ord-be840b94b3cb41d78632752614fbfae4 |
| Source note | uspto-grants-1996_10 |