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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 865965Generated: October 31, 2026

p-Toluenesulfonic acid → HCID 19047547, compound

https://huagongshe.com/reaction/865965

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantHCID 19047540HCID 19047540—
SolventTolueneHCID 1140—
ProductHCID 19047547HCID 1904754761.7%

Reaction Steps

To a mixture of 5 g (0.024 mol) of 1-(3-furyl)-indan-1-ol in 500 ml of toluene was added 50 mg of p-toluenesulfonic acid and the mixture was placed on a Rotovap® and the solvent was distilled in vacuo (40 mm) until a residue was obtained. The residue was chromatographed (silica, 1:1 hexane/methylene chloride) to afford 2.7 g (61.3%) of 1-(3-furyl)-indene as a clear oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05569655
Source datasetuspto-grants-1996_10
ORD IDord-0625321083b64b389b215709cbf0fe34
Source noteuspto-grants-1996_10