Dichloroacetyl chloride → HCID 885713, compound

HRID 866310Notes

Reaction equation

HRID 866310 reaction equation
[CH:1]1[CH:6]=[CH:5][C:4]([NH:7][C:8]2[CH:13]=[CH:12][C:11]([NH2:14])=[CH:10][CH:9]=2)=[CH:3][CH:2]=1.[Cl:15][CH:16]([Cl:20])[C:17](Cl)=[O:18]>>[NH:7]([C:8]1[CH:13]=[CH:12][C:11]([NH:14][C:17](=[O:18])[CH:16]([Cl:20])[Cl:15])=[CH:10][CH:9]=1)[C:4]1[CH:3]=[CH:2][CH:1]=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 6593Dichloroacetyl chlorideHCID 7564N-Phenyl-p-phenylenediamine

Product 1

HCID 885713HCID 885713, compound

Procedure

This compound is prepared from 4-aminodiphenylamine (36.8 g) in the same manner as Compound 1, except that dichloroacetyl chloride (29.8 g) is used in place of trichloroacetyl chloride. The product is recrystallized from benzene. The m.p. and chemical analysis are reported in Table I.

Workup

  1. customThe product is recrystallized from benzene

Sources & evidence

ORD record
ord-59176ed2b3034908b10f33119d7d4952
Source dataset
uspto-grants-1978_07
Patent number
US04098760

Reaction notes

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