HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 12878607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Glycinamide hydrochloride | HCID 2723639 | — |
| Reactant | 2-[3-(Dimethylamino)propoxy]benzaldehyde | HCID 2995968 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12878607 | HCID 12878607 | 93.9% |
Reaction Steps
Fifteen grams of 2-(3-dimethylaminopropoxy)benzal-dehyde and 8.1 g of glycinamide, hydrochloride are reacted in 300 ml of ethanol in the presence of 4.8 g of 85% potassium hydroxide as described in Example 1 to give 20 g of a crude semi-solid product. The crude product is triturated with 100 ml of isopropyl ether and cooled to yield 17.9 g of solid; melting point 71-73° C (sintering at 60° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04098789 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-ab63475e03914f01bd522a9aaf957847 |
| Source note | uspto-grants-1978_07 |