HRID866378

反应详情

EQUATION

反应方程式

HRID 866378 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 4-cyanophenoxy phenyl methane (10.45g.; 0.05 mole), 30% hydrogen peroxide (20ml) and 6N NaOH (20ml) and ethanol (30ml) was maintained at 40°-50° for 3 hrs., cooled and neutralised. The product was filtered off and recrystallised from ethanol M.p. 186°-7°.

WORKUP

后处理

  1. temperaturewas maintained at 40°-50° for 3 hrs
  2. temperature, cooled
  3. filtrationThe product was filtered off
  4. customrecrystallised from ethanol M.p. 186°-7°