HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86734035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | 4-Benzyloxybenzoylchloride | HCID 3766410 | — |
| Product | HCID 86734035 | HCID 86734035 | — |
Reaction Steps
A mixture of cyclohexylamine (3.6g.; 0.036 mole) and 4-chlorocarbonylphenoxy phenyl methane (9.04g.; 0.037 mole) in pyridine were heated under reflux for 6hr., then poured into water. The product was extracted into dichloromethane, the organic layer washed with dil. HCl and dried (anhyd. MgSO4). Removal of the drying agent and solvent yielded the crude product which was recrystallised from ethanol M.p. 183°-4°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04098816 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-df50c2d210844c839a4d5c286909894f |
| Source note | uspto-grants-1978_07 |