Sodium Iodide → HCID 20320786, compound

HRID 866393Notes

Reaction equation

HRID 866393 reaction equation
Cl/[CH:2]=[CH:3]/[C:4]([CH:6]1[CH2:11][CH2:10][C:9]2([CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]2)[CH2:8][CH2:7]1)=[O:5].[I-:17].[Na+]>CC(C)=O>[I:17]/[CH:2]=[CH:3]/[C:4]([CH:6]1[CH2:11][CH2:10][C:9]2([CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]2)[CH2:8][CH2:7]1)=[O:5]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 20320773HCID 20320773, compound

Product 1

HCID 20320786HCID 20320786, compoundYield 70.9%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

In a procedure as described in Example 9H, 1-chloro-3-(spiro[5.5]undec-3-yl)-1E-propen-3-one was reacted with sodium iodide in acetone to yield 1-iodo-3-(spiro[5.5]undec-3-yl)-1E-propen-3-one (70.9%).

Sources & evidence

ORD record
ord-76f24399b4ef4ed5ba579df55e2aef82
Source dataset
uspto-grants-1978_07
Patent number
US04098823

Reaction notes

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