Sodium Iodide → HCID 20320792, compound

HRID 866398Notes

Reaction equation

HRID 866398 reaction equation
Cl/[CH:2]=[CH:3]/[C:4]([C:6]1([CH3:13])[CH2:9][C:8]2([CH2:12][CH2:11][CH2:10]2)[CH2:7]1)=[O:5].[I-:14].[Na+]>CC(C)=O>[I:14]/[CH:2]=[CH:3]/[C:4]([C:6]1([CH3:13])[CH2:9][C:8]2([CH2:12][CH2:11][CH2:10]2)[CH2:7]1)=[O:5]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 20320785HCID 20320785, compound

Product 1

HCID 20320792HCID 20320792, compoundYield 87%

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

In a procedure as described in Example 9H, 1-chloro-3-(2-methylspiro[3.3]hept-2-yl)-1E-propen-3-one was reacted with sodium iodide in acetone to yield 1-iodo-3-(2-methyspiro[3.3]hept-2-yl)-1E-propen-3-one (87%).

Sources & evidence

ORD record
ord-52f798989dc34b00a0e4249ff62b579c
Source dataset
uspto-grants-1978_07
Patent number
US04098823

Reaction notes

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