Ethylamine → HCID 20321048, compound

Participants

Reaction Steps

A mixture of 500 mg. of methyl 2-nitroisonicotinate and 2 ml. of 70% ethylamine was stirred at room temperature for 5 hours. The reaction mixture was extracted with ethyl acetate. The extract was washed with water, dried and then the solvent was distilled off. The crystalline residue was recrystallized from ethyl acetate-n-hexane to give 328 mg. of the desired product.

Provenance & Evidence