1-Methylpiperazine → HCID 54412511, compound

HRID 866621Notes

Reaction equation

HRID 866621 reaction equation
CN1CCNCC1.[Cl:8][C:9]1[CH:10]=[CH:11][C:12]2[CH:18]=[C:17]([N:19]3CCN(C)CC3)[C:16]3[CH:26]=[CH:27][C:28]([C:30]([F:33])([F:32])[F:31])=[CH:29][C:15]=3[O:14][C:13]=2[CH:34]=1>>[Cl:8][C:9]1[CH:10]=[CH:11][C:12]([CH2:18][C:17]#[N:19])=[C:13]([O:14][C:15]2[CH:16]=[CH:26][CH:27]=[C:28]([C:30]([F:31])([F:32])[F:33])[CH:29]=2)[CH:34]=1

Participants

3

Reactant 2

HCID 531671-MethylpiperazineHCID 22767875HCID 22767875, compound

Product 1

HCID 54412511HCID 54412511, compound

Procedure

The last-named intermediate is reacted with 1-methylpiperazine in the same manner as described in Example 14 to give the desired starting material, 1-[3-chloro-7-trifluoromethyl-dibenz[b,f]oxepin-10-yl]-4-methylpiperazine, having a melting point of 170° C.

Workup

  1. customto give the

Sources & evidence

ORD record
ord-2c8ec30a3a49483e980e52163eb882e9
Source dataset
uspto-grants-1978_07
Patent number
US04100173

Reaction notes

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