Methyl Isocyanate → HCID 54506864, compound

Participants

Reaction Steps

To a solution of 16.8 g of crude 2-oximino-3,3-dimethyl-1,4-dioxane and 2 drops of triethylamine was added 17 ml of methyl isocyanate. The reaction mixture was left at ambient temperature for 16 hours. The reaction mixture was concentrated and filtered to yield 4.0 g of 3,3-dimethyl-2-[O-(methylcarbamoyl)oximino]-1,4-dioxane, m.p. 144°-146° C. (m/e 202).

Provenance & Evidence