HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl hydroperoxide → HCID 20318133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | 2-Propanol, 2-[(1,1-dimethylethyl)azo]- | HCID 94582 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | 55296-56-5 | HCID 15644349 | — |
| Reactant | HCID 20393238 | HCID 20393238 | — |
| Product | HCID 20318133 | HCID 20318133 | — |
Reaction Steps
Crude 2-t-butylazo-2-butylperoxypropane was prepared by reacting 2-t-butylazo-2-chloropropane with an aqueous solution of the potassium salt of t-butyl hydroperoxide according to the method described in MacLeay, Lange and Sheppard application Ser. No. 426,411 filed Dec. 19, 1973, (which is incorporated herein by reference). The resultant product contained approximately 75% 2-t-butylazo -2-t-butylperoxypropane and 25% 2-t-butylazo-2-hydroxy-propane (which has been marketed as "LUCEL 3").
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101464 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-febbb632064a424f962542299057cc68 |
| Source note | uspto-grants-1978_07 |