Oxalyl chloride → HCID 12298995, compound

HRID 866762Notes

Reaction equation

HRID 866762 reaction equation
[CH3:1][C:2]1[S:6][N:5]=[N:4][C:3]=1[C:7]([O:9]CC)=O.C(Cl)(=O)C([Cl:15])=O>>[CH3:1][C:2]1[S:6][N:5]=[N:4][C:3]=1[C:7]([Cl:15])=[O:9]

Participants

3

Reactant 2

HCID 65578Oxalyl chlorideHCID 351614Ethyl 5-methyl-1,2,3-thiadiazole-4-carboxylate

Product 1

HCID 12298995HCID 12298995, compound

Procedure

Hydrolysis of ethyl 5-methyl-1,2,3-thiadiazole-4-carboxylate (D. L. Pain and R. Slack, J. Chem. Soc., 5166 (1965)) and subsequent treatment of the acid with oxalyl chloride according to the method of Example 3 provides 5-methyl-1,2,3-thiadiazole-4-carbonyl chloride.

Sources & evidence

ORD record
ord-785c63089b42454cb1d2ca7ddfb18ead
Source dataset
uspto-grants-1978_07
Patent number
US04101548

Reaction notes

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