HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 519133, compound → HCID 70618756, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 519133 | HCID 519133 | — |
| Reactant | HCID 178478191 | HCID 178478191 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 70618756 | HCID 70618756 | — |
Reaction Steps
Bis(p-chlorophenyl)propylphosphine was prepared by reacting 0.2 mole of propyldichlorophosphine with 0.4 mole of p-chlorophenylmagnesium bromide. The product was isolated by chloroform extraction and distillation as previously described. The portion boiling between 160° and 165° C. under a pressure of 2 mm. Hg was collected. The analysis corresponded to bis(p-chlorophenyl)propylphosphine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101655 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-3f9073a68f8240ffbf241315bc49eaa1 |
| Source note | uspto-grants-1978_07 |