HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22762753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-(Chloromethyl)-5-(4-chlorophenyl)-1,3-oxazole | HCID 736966 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22762753 | HCID 22762753 | 71% |
Reaction Steps
A suspension of 2.3 g of 2-chloromethyl-5-(4-chlorophenyl) oxazole and 1.94 g of potassium phthalimide in 15 ml of dimethylformamide was stirred at room temperature for one hour. The reaction mixture was poured into 300 ml of water, and the resultant precipitate was filtered and recrystallized from ethanol to give 2.4 g (71 percent) of N-[5-(4-chlorophenyl)-2-oxazolyl]methylphthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101660 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-2c11c45f037d45448040d4a98aeb33bb |
| Source note | uspto-grants-1978_07 |