HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 18925560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 21312345 | HCID 21312345 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18925560 | HCID 18925560 | — |
Reaction Steps
A solution of 22 g (0.092 mole) of 4-methylbenzhydrylisothiocyanate in 250 ml of dry ether at 0° is treated with anhydrous NH3 for 3 hours while stirring. The mixture is stirred an additional 1.5 hours at 0° to 10° C during which time the crude product precipitates as a white solid. Filtration and washing with Et2O affords the product; mp 167°-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101659 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-b38774d4bd574178b8c3d56ed63ba0ad |
| Source note | uspto-grants-1978_07 |