HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 2-Amino-N,N-diethyl-5-methoxy-benzylamine | HCID 422009 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine | HCID 20319240 | — |
Reaction Steps
2-Amino-3-bromo-N,N-diethyl-5-methoxy-benzylamine was prepared from 2-amino-N,N-diethyl-5-methoxy-benzylamine and bromine analogous to Example 9. Proof of structure by IR-, UV- and NMR-spectra. IR-spectrum (methylenechloride): 3250 cm-1NH2 ; 3410 cm-1NH2 ; 2830 cm-1OCH3 ; 2800 cm-1N-ethyl; 1480 cm-1C=C; 1590 cm-1C=C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04101671 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-dfa5916725ad4205abe48c5ad5157beb |
| Source note | uspto-grants-1978_07 |