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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 866987Generated: October 30, 2026

Thionyl Chloride → HCID 22750308, compound

https://huagongshe.com/reaction/866987

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 22750325HCID 22750325—
ReactantHCID 22750339HCID 22750339—
SolventDimethylformamideHCID 6228—
ProductHCID 22750308HCID 22750308—

Reaction Steps

From 7.0 g. of 6-[4-(2-pyridylaminosulfonyl)phenyl]-1,2-dihydro-2-oxonicotinic acid in 200 ml. of thionyl chloride, and 1.5 ml. of dimethylformamide, following the procedure of (c) above, there is obtained 6-[4-(2-pyridylaminosulfonyl)phenyl]-1,2-dihydro-2-oxonicotinyl chloride hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04101661
Source datasetuspto-grants-1978_07
ORD IDord-3794cb1fd18d4136aabc704ef68abf69
Source noteuspto-grants-1978_07