HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 13020124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 13020116 | HCID 13020116 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13020124 | HCID 13020124 | — |
Reaction Steps
0.8 g (2.5 mmole) of ethyl 3-(4-bromophenyl)-3-hydroxy-3-(3-pyridyl)-propanoate, 50 ml of aqueous ammonia and 10 ml of absolute ethanol was stirred at room temperature for 24 hours. The white precipitate obtained was collected by filtration. Recrystallization from isopropyl alcohol gave 0.45 g (56%), m.p. 213°-214° C. The formula C14H13BrN2O2 was verified through elemental analysis, C calculated 52.4, found 51.9. ##STR30##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04102887 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-22d7d7c763f9494fbb0e8f7eca0579fc |
| Source note | uspto-grants-1978_07 |