HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(1-Acetyloxycyclohexyl)-3-benzyloxy-1-propyne → 3-(1-Acetyloxycyclohexyl)-1-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(1-Acetyloxycyclohexyl)-3-benzyloxy-1-propyne | HCID 20317376 | — |
| Reactant | Benzyl 7-{2-(3-benzyloxy-4-[4-fluorophenoxy]butyl)-1,1,4-trioxo-3-thiazolidinyl}heptanoate | HCID 20317381 | — |
| Product | 3-(1-Acetyloxycyclohexyl)-1-propanol | HCID 20317384 | — |
Reaction Steps
This compound is prepared essentially by the method as described in Example 4, Step E, except that the benzyl 7-{2-(3-benzyloxy-4-[4-fluorophenoxy]butyl)-1,1,4-trioxo-3thiazolidinyl}heptanoate is replaced by 1-(1-Acetyloxycyclohexyl)-3-benzyloxy-1-propyne and no chromatographic purification is needed. The title compound is obtained as an essentially colorless, mobile liquid which is used immediately in Step A-3 below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04102888 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-902dbe8e14374e0eb436538d476784f9 |
| Source note | uspto-grants-1978_07 |