HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 7-{2-(3-benzyloxy-4-[4-fluorophenoxy]butyl)-1,1,4-trioxo-3-thiazolidinyl}heptanoate → 4(S)acetyloxy-1-nonanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 7-{2-(3-benzyloxy-4-[4-fluorophenoxy]butyl)-1,1,4-trioxo-3-thiazolidinyl}heptanoate | HCID 20317381 | — |
| Reactant | 1-benzyloxy-4(S) acetyloxy-2-nonyne | HCID 22800252 | — |
| Product | 4(S)acetyloxy-1-nonanol | HCID 22800255 | — |
Reaction Steps
This compound is prepared essentially by the method as described in Example 5, Step E, except that the benzyl 7-{2-(3-benzyloxy-4-[4-fluorophenoxy]butyl)-1,1,4-trioxo-3-thiazolidinyl}heptanoate is replaced by 1-benzyloxy-4(S) acetyloxy-2-nonyne and no chromatographic purification is needed. The title compound is obtained as a mobile oil which is used immediately in Step A-6 below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04102888 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-b0783204581c4619a9a132188c1e307b |
| Source note | uspto-grants-1978_07 |