HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178435618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 10563642 | HCID 10563642 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178435618 | HCID 178435618 | — |
Reaction Steps
3-Cyano-7-ethylthioxanthone (5.3 g), sodium azide (1.55 g), and ammonium chloride (1.26 g) in dimethylformamide were heated at 120° C. for 3 hours, cooled, and poured into dilute hydrochloric acid. The solid precipitate was filtered off and recrystallised twice from acetic acid to yield 7-ethyl-3-(5-tetrazolyl)thioxanthone m.p. 247° C. with decomposition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04103015 |
| Source dataset | uspto-grants-1978_07 |
| ORD ID | ord-27ba1eff69cf46f5ab1b3db91cc73e23 |
| Source note | uspto-grants-1978_07 |