Thionyl Chloride → HCID 10540931, compound

Participants

Role	Name	HCID	Charge
Reactant	Thionyl Chloride	HCID 24386	—
Reactant	7-Methyl-9,10,10-trioxo-9,10-dihydro-10lambda~6~-thioxanthene-3-carboxamide	HCID 20317794	—
Solvent	Dimethylformamide	HCID 6228	—
Product	HCID 10540931	HCID 10540931	—

Reaction Conditions

Temperature	-10 °C

Reaction Steps

The amide (0.79 g) of Example 21 was added to a mixture of dimethyl formamide (100 ml) and thionyl chloride (2.0 ml) at -10° C., and stirred at -10° C. for 2 hrs. The mixture was poured on to ice-water and the precipitated product filtered off and washed with water, recrystallised from dimethylformamide, and dried at 155° C./15 mm. Hg, m.p. 290° C. (decomposes).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04103015
Source dataset	uspto-grants-1978_07
ORD ID	ord-c462b2931d014b478af8cc54973dcf9d
Source note	uspto-grants-1978_07