HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 14032515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 178480237 | HCID 178480237 | — |
| Product | HCID 14032515 | HCID 14032515 | 62.2% |
Reaction Steps
A mixture of 3.0 g of 3-(1-methyl-4-piperidinyl)-1H-indazole and 3.2 ml of benzoyl chloride was heated at 100° for 2 hrs. The resultant solid was triturated with ether and collected. The salt was twice recrystallized from ethanol-ether to yield 3.1 g (62.2%) of product, mp 234°-236° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04775761 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-358be1df674d4828a9838ab6f1f433e5 |
| Source note | uspto-grants-1988_10 |