Water → HCID 22133497, compound

Participants

Reaction Steps

30.2 g of dimethyl carbonate, 62.1 g of tri-n-butylamine, 30.5 g of water and 15.0 g of methanol were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 140° C., the reaction was continued for 7 hours at 140° C. Tributylammonium hydrogencarbonate was obtained in a yield of 84.3 mol % (based on tri-n-butylamine).

Provenance & Evidence