HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-{3-[2-(4-Propyl-piperidin-1-yl)-ethoxy]-phenyl}-thieno[2,3-d]isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Propylpiperidine | HCID 31169 | — |
| Reactant | 3-[3-(2-Bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole | HCID 21983582 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3-{3-[2-(4-Propyl-piperidin-1-yl)-ethoxy]-phenyl}-thieno[2,3-d]isoxazole | HCID 21983562 | — |
Reaction Steps
The title compound is prepared from 3-[3-(2-bromo-ethoxy)-phenyl]-thieno[2,3-d]isoxazole, potassium carbonate, 4-N-propylpiperidine and acetonitrile essentially as described above in example 40. Purity by LC/MS (APCI)=96%, [M+H]+=371.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091199B1 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-00713097cc4a4a48b60bcfb12597d27b |
| Source note | uspto-grants-2006_08 |