Sodium Hydroxide → HCID 14271000, compound

Participants

Reaction Steps

A solution of 1-(3-thienylcarbonyl)pyrrolidine (12 g) in dry diethylether (200 ml) was added to a slurry of lithium aluminium hydride (2.6 g) in dry diethylether (100 ml). The mixture was stirred for 1 hour, and aqueous 5M sodium hydroxide (20 ml) was added. The mixture was filtered and the filtrate was distilled to give the title compound (9.8 g) as a colourless oil b.p. 120/15 mm.

Provenance & Evidence