Hydrazine hydrate (1:1) → HCID 12926539, compound

Participants

Reaction Steps

N-[3-[[5-(Dimethylamino)methyl-4-methyl-2-thienyl]thio]propyl]isoindole-1,3(2H)-dione (15.2 g) and hydrazine hydrate (8 ml) were stirred at room temperature in tetrahydrofuran (150 ml) for 48 h. The mixture was filtered and the filtrate was distilled to give the title compound as an orange oil (6.9 g) b.p. 160°-170°/0.04 mm.

Provenance & Evidence