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HRID867944

反应详情

EQUATION

反应方程式

HRID 867944 的结构方程式

REACTANTS

反应物

2
结构：NCCc1ccccn1
HCID75919

2-(2-Aminoethyl)pyridine

C7H10N2

结构：CC12CCC(C(=O)OC1=O)C2(C)C
HCID94834

1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione

C10H14O3

PRODUCTS

生成物

1
结构：CC12CCC(C(=O)N(CCc3ccccn3)C1=O)C2(C)C
HCID14235066

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

A mixture of (-) camphoric anhydride 5 g (0.029 mol), 2-(2-aminoethyl)pyridine 3.6 (0.03 mol) and 50 ml of pyridine was refluxed overnight. The solvent is removed under reduced pressure and the remaining oil boiled in 20 ml of ethanol and allowed to cool.

WORKUP

后处理

  1. temperaturewas refluxed overnight
  2. customThe solvent is removed under reduced pressure
  3. temperatureto cool