HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21289506, compound → HCID 21289505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21289506 | HCID 21289506 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21289505 | HCID 21289505 | 99.3% |
Reaction Steps
1.8 g of ethyl 6-(3-pyridylmethyl)-7,8-dihydro-2-naphthalenecarboxylate was dissolved in 100 ml of ethanol and 1 g of 10% palladium carbon was added thereto. The mixture was catalytically reduced. After absorption of hydrogen gas was completed, the catalyst was removed by filtration. The filtrate was concentrated in vacuo to give 1.8 g of ethyl 6-(3-pyridylmethyl)-5,6,7,8-tetrahydro-2-naphthalenecarboxylate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04777257 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-567dd333a0aa4a88a90c93d7c9b0f635 |
| Source note | uspto-grants-1988_10 |