Hydrochloric Acid → HCID 70388211, compound

Participants

Reaction Steps

1.3 g of ethyl 6-(1-imidazolylmethyl)-5,6,7,8-tetrahydro-2-naphthalenecarboxylate was mixed with 15 ml of a 5% solution of hydrogen chloride in ethanol, and the mixture was concentrated to dryness in vacuo. The residue was recrystallized from a mixture of isopropanol and diethyl ether to give 1.2 g of ethyl 6-(1-imidazolylmethyl)-5,6,7,8-tetrahydro-2-naphthalenecarboxylate hydrochloride as colorless crystals with m.p. 180°-182° C.

Provenance & Evidence