HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13800023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Ethyl Beta-Carboline-3-Carboxylate | HCID 105078 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 13800023 | HCID 13800023 | — |
Reaction Steps
400 mg of AlCl3 was suspended in 10 ml of acetyl chloride at 0° C. and 600 mg of beta-carboline-3-carboxylic acid ethyl ester was added. After 5 minutes, 600 mg of AlCl3 was added and the mixture was stirred for 1 hour. Alcohol was added and the pH adjusted to 7-8. 50 ml of water was added and the filtered mixture yielded 450 mg of raw product, which was recrystallized from ethanol/water (1:1). Mp: 290°-305° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04778800 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-c0c039efad8c487cb3c3076ff4d77d06 |
| Source note | uspto-grants-1988_10 |