HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14444197, compound → 3-Pyridinecarboxaldehyde, 6-(1-methylethyl)- (9CI)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14444197 | HCID 14444197 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-Pyridinecarboxaldehyde, 6-(1-methylethyl)- (9CI) | HCID 14444198 | 73.5% |
Reaction Steps
To a solution of 5.1 g of 5-hydroxymethyl-2-isopropylpyridine in 70 ml of chloroform, 20 g of active manganese dioxide is added, and the mixture is refluxed with stirring for 1 hour. The insoluble manganese dioxide is filtered off, and the filtrate is concentrated to give 3.7 g of crude 6-isopropyl-3-pyridinecarbaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04778796 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-5c0534d385a44583b88a0521eb4ff4c2 |
| Source note | uspto-grants-1988_10 |