HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54287949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 2-Bromobenzaldehyde | HCID 81129 | — |
| Product | HCID 54287949 | HCID 54287949 | 90% |
Reaction Steps
2-Bromobenzaldehyde (0.09 mol) was then added in tetrahydrofuran (25 mL) and after the mixture had been stirred for a further 30 min at 0° C. hexane and aqueous methanol (40:60) was added. The hexane extract was concentrated and the residue was distilled to yield 2-(1-decenyl)-1-bromobenzene (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780251 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-043781c8028148d0a262e43415ab26aa |
| Source note | uspto-grants-1988_10 |