Methanol → HCID 54287949, compound

HRID 868488Notes

Reaction equation

HRID 868488 reaction equation
[Br:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=O.[CH3:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].CO.O1C[CH2:21][CH2:20][CH2:19]1>>[CH:4]([C:3]1[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=1[Br:1])=[CH:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:19][CH2:20][CH3:21]

Participants

5

Reactant 4

HCID 887MethanolHCID 8028TetrahydrofuranHCID 8058HexaneHCID 811292-Bromobenzaldehyde

Product 1

HCID 54287949HCID 54287949, compoundYield 90%

Procedure

2-Bromobenzaldehyde (0.09 mol) was then added in tetrahydrofuran (25 mL) and after the mixture had been stirred for a further 30 min at 0° C. hexane and aqueous methanol (40:60) was added. The hexane extract was concentrated and the residue was distilled to yield 2-(1-decenyl)-1-bromobenzene (90%).

Workup

  1. additionwas added
  2. extractionThe hexane extract
  3. concentrationwas concentrated
  4. distillationthe residue was distilled

Sources & evidence

ORD record
ord-043781c8028148d0a262e43415ab26aa
Source dataset
uspto-grants-1988_10
Patent number
US04780251

Reaction notes

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