HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethoxyphenol → HCID 14886366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethoxyphenol | HCID 7041 | — |
| Reactant | Ethylene carbonate | HCID 7303 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 14886366 | HCID 14886366 | 100.7% |
Reaction Steps
A mixture of 6.0 g of 2,6-dimethoxyphenol, 6.8 g of ethylene carbonate and 5.4 g of potassium carbonate in 40 ml of toluene was refluxed for 17 hours. After cooling, toluene solution was separated, dried (Na2SO4) and solvent was evaporated. 7.77 g of desired compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04780462 |
| Source dataset | uspto-grants-1988_10 |
| ORD ID | ord-6f57dac6ec1f4290a78e514474cafdc2 |
| Source note | uspto-grants-1988_10 |